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LP auto-MATE低压多釜全自动反应系统

上海堪鑫仪器设备有限公司
会员指数: 企业认证:

价格:电议

所在地:上海

型号:

更新时间:2016-07-13

浏览次数:1520

公司地址:上海市浦东新区合庆镇华夏东路3220号

尧先生(先生) 主管 

产品简介

LP auto-MATE The auto-MATE is a miniature (>50ml) computer controlle

公司简介

  上海堪鑫仪器设备有限公司是一家专业从事科学仪器与设备研究、开发、生产、组装与经营的生产型为主的企业,主攻产品为从实验室研究及小试到生产车间中试及小生产相关的化学合成反应器及周遍设备及安全和监测仪器等,致力于从半自动控制到全自动控制,从微型容量到中等规模容量的反应及监控设备的开发于生产,吸收国内外同业所长,结合国内研究与生产实际,努力于发展成为该行业国内第一品牌。其他生产的产品包括平行合成仪、低温循环制冷泵、加热冷却循环水油槽、高低温水油浴、自动导热油水冷装置、振荡器、振荡机恒温摇床(振荡培养箱)、恒温金属浴、二恒及三恒电泳仪、发酵罐专用补料瓶、防漏塑料试剂瓶等。

  公司研究开发与市场推广基地位于上海市浦东新区张江高科技园区,生产组装基地位于上海市嘉定区南翔高科技经济园区。

  经营范围:

  1)以西安交通大学先进制造技术研究所与华东理工大学生化工程研究所为技术支撑,致力于自主知识产权的生物与化工仪器设备产品的自动控制研究开发和实践应用推广。

  2)专业代理世界顶级品牌科学仪器、工业质检仪器,相关消耗品及国产品牌理化实验设备,包括分析测试仪器,化工研究、中试、生产设备,生化研究器材,实验室通用仪器及耗材等四大系列,并承接仪器设备组配业务。专业涉及生命科学、医学、制药、环保、农业、食品、饮料、日用化学、化妆品及轻工化工、在国内具有广泛的客户基础和良好的商业信誉。

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产品说明

LP auto-MATE The auto-MATE is a miniature (>50ml) computer controlled multiple reactor (parallel synthesis) system designed for optimisation of batch and semi-batch chemical processes. auto-MATE is a powerful system that includes the best features associated with bench scale reactors and robotic systems. Virtually any chemistry that can also be done on the litre scale can be carried out in the auto-MATE. It is the only system where experiments can be performed under realistic plant conditions (agitation, feed etc), fully automated and controlled, using miniature reactors running independently from a single PC. auto-MATE offers you the opportunity to carry out large numbers of experiments in the shortest possible time, allowing process optimisation in days NOT months. Process conditions can be controlled and monitored simultaneously in multiple reactors at one time with independent control of all conditions (e.g. temperature, reagent feed, agitation). It is also an ideal complement to robotic units that can identify large numbers of candidate reactions, but are unable to identify key reaction parameters. auto-MATE is able rapidly to eliminate the impractical options identified by robotic systems and then assist in generating practical and viable processes. Experimental Design Made Simple: The successful application of experimental design to process development involves performing a series of experiments with precise control of key variables. • Multiple systems controlled through a single PC • Fully independent operational conditions: temperature / feed rates, etc • Automated reactor sampling options • WALKAWAY operation (24 hr throughput) • >50ml sample volume • Fully automated control of reactor conditions: feed rates / temperature / pressure / agitation • High pressure options (up to 200 bar) • Specialist construction materials: glass / stainless steel / Hastelloy / PTFE Specification... Specification Complete Units: Each unit consists of a thermostatically controlled oil jacket into which a reactor is in-serted. The reactor cover, complete with stirrer, temperature probe etc, can be lowered onto the reactor and easily secured to provide a tight seal, ready for chemical addition. Each reactor includes a dedicated stirrer, thermocouple, heater, three additional ports for feeds and other probes. Each parameter, including reactor temperature, feed rate, sequence of steps (heat, cool, dose etc), are set independently using the winISO™ software. Reactors: The unique interchangeable reactor system of the auto-MATE™ allows study of the most demanding of chemistries on one unit. Glass and metal reactors simulate real plant conditions For highly reactive chemicals, such as hydrogen fluoride, PTFE construction is available. Examples of reactions studied to date include hydrogenation, nitration, and even HF chemistries. Operating Range: From vacuum pressure to 200 bar, from 30 to 100ml, between -80 and 350oC, and even reflux experiments. Sampling: In many applications, samples for analysis can be taken at the end of the experiment. Where intermediate samples are needed, the procedure can be automated by use of either stand-alone sampling unit, or else, by integrating a robot with the auto-MATE. HEL has developed proprietary techniques for both these options. Parallel Processing: auto-MATE™ is typically supplied in units of four reactors, run from the same computer. Each reactor can be at different temperatures, performing different operations, which can be started/stopped independently. Alarms and safety conditions for each reactor can individually be specified to allow for 24 hour unattended operation. Feeds: auto-MATE™ can deal with liquid feeds using a syringe, peristaltic, piston, HPLC or pump/balance combination. Gas feeds are also possible, controlled on mass flow and/or reactor pressure. Even dosing of solids is possible using a new design of screw feeder. For complex systems with large number of feeds, manifolds with automatic routing, can be used to reduce the number of pumps necessary. Temperature Control: Independent and precise, each reactor is totally autonomous. Thermal Trending and Calorimetry: Quantitative power compensation calorimetry to give additional insight into reaction progress. HPLC Integration For a complete solution, an HPLC unit can also be fully integrated. The results of the analysis can be used in real time - to define the operation of the AUTO-LAB.
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